Evaluating a Dispersion of Sodium in Sodium Chloride for the Synthesis of Low?Valent Nickel Complexes
نویسندگان
چکیده
The use of a sodium in chloride dispersion is systematically evaluated for the synthesis nickel(0) and nickel(I) complexes from readily-prepared nickel(II) precursors. A variety with phosphine bipyridine-type ligands were accessed, although some reactions found to produce mixtures nickel(I), yields highly variable. Several new obtained, these characterized using techniques including NMR spectroscopy, EPR single crystal X-ray diffraction analysis.
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ژورنال
عنوان ژورنال: European Journal of Inorganic Chemistry
سال: 2021
ISSN: ['1434-1948', '1099-0682']
DOI: https://doi.org/10.1002/ejic.202101006